Synthesis and reduction of 10-phthalimidocamphor oxime

Uroš Grošelj, Amalija Golobič, Jurij Svete, Sebastijan Ričko

Abstract


10-Phthalimidocamphor oxime was prepared from easily available 10-iodocamphor in two steps. Reduction of the oxime functionality resulted in the formation of two novel polycyclic isoindolinone heterocycles, the attempted preparation of the primary amine failed. The structures of novel heterocycles were unambiguously confirmed by single crystal X-ray diffraction as well as NMR techniques.

Keywords


10-iodocamphor; 10-phthalimidocamphor oxime; camphor derived amines; reduction

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DOI: http://dx.doi.org/10.17344/acsi.2017.3474

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